Atomic force microscopy at ambient and liquid conditions with stiff sensors and small amplitudes

Wutscher, Elisabeth and Giessibl, Franz J. (2011) Atomic force microscopy at ambient and liquid conditions with stiff sensors and small amplitudes. REVIEW OF SCIENTIFIC INSTRUMENTS, 82 (9): 093703. ISSN 0034-6748,

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Abstract

We report on atomic force microscopy (AFM) in ambient and liquid environments with the qPlus sensor, a force sensor based on a quartz tuning fork with an all-electrical deflection measurement scheme. Small amplitudes, stiff sensors with bulk diamond tips and high Q values in air and liquid allow to obtain high resolution images. The noise sources in air and liquid are analyzed and compared for standard silicon cantilevers and qPlus sensors. First, epitaxial graphene was imaged in air, showing atomic steps with 3 angstrom height and ridges. As a second sample system, measurements on calcite (CaCO3) in liquids were performed in water and polyethylenglycol (PEG). We demonstrate high resolution images of steps in PEG on calcite and nanolithography processes, in particular with frequency-modulation AFM the controlled dissolution of calcite monolayers. (C) 2011 American Institute of Physics. [doi:10.1063/1.3633950]

Item Type: Article
Uncontrolled Keywords: QUARTZ TUNING FORK; AQUEOUS-SOLUTION; CALCITE GROWTH; DIAMOND TIPS; SURFACE; DISSOLUTION; RESOLUTION; AFM; LITHOGRAPHY; CANTILEVERS; atomic force microscopy; calcium compounds; diamond; force sensors; graphene; noise; Q-factor; quartz; vibrations
Subjects: 500 Science > 530 Physics
Divisions: Physics > Institute of Experimental and Applied Physics > Chair Professor Giessibl > Group Franz J. Giessibl
Depositing User: Dr. Gernot Deinzer
Date Deposited: 02 Jun 2020 08:33
Last Modified: 02 Jun 2020 08:33
URI: https://pred.uni-regensburg.de/id/eprint/20237

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