Preparation of light-atom tips for scanning probe microscopy by explosive delamination

Hofmann, Thomas and Welker, J. and Giessibl, F. J. (2010) Preparation of light-atom tips for scanning probe microscopy by explosive delamination. JOURNAL OF VACUUM SCIENCE & TECHNOLOGY B, 28 (3). ISSN 1071-1023,

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Abstract

To obtain maximal resolution in scanning tunneling microscopy (STM) and atomic force microscopy, the size of the protruding tip orbital has to be minimized. Beryllium as tip material is a promising candidate for enhanced resolution because a beryllium atom has just four electrons, leading to a small covalent radius of only 96 pm. Besides that, beryllium is conductive and has a high elastic modulus, which is a necessity for a stable tip apex. However, beryllium tips that are prepared ex situ are covered with a robust oxide layer, which cannot be removed by just heating the tip. Here, the authors present a successful preparation method that combines the heating of the tip by field emission and a mild collision with a clean metal plate. That method yields a clean, oxide-free tip surface as proven by a work function of Phi(expt)=5.5 eV as deduced from a current-distance curve. Additionally, a STM image of the Si-(111)-(7x7) is presented to prove the single-atom termination of the beryllium tip. (C) 2010 American Vacuum Society. [DOI: 10.1116/1.3294706]

Item Type: Article
Uncontrolled Keywords: FORCE MICROSCOPY; WORK FUNCTION; BERYLLIUM; SILICON; VACUUM; atomic force microscopy; beryllium; delamination; field emission; scanning tunnelling microscopy; work function
Subjects: 500 Science > 530 Physics
Divisions: Physics > Institute of Experimental and Applied Physics > Chair Professor Giessibl > Group Franz J. Giessibl
Depositing User: Dr. Gernot Deinzer
Date Deposited: 03 Aug 2020 06:35
Last Modified: 03 Aug 2020 06:35
URI: https://pred.uni-regensburg.de/id/eprint/24789

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