Kaiser, Jens and Mekic, Amel and Parham, Amir Hossain and Buchholz, Herwig and Koenig, Burkhard (2020) Synthesis and Characterization of Naphtho[2,1-b:7,8-b ']bis[1]benzothiophene. EUROPEAN JOURNAL OF ORGANIC CHEMISTRY (1). pp. 66-69. ISSN 1434-193X, 1099-0690
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We describe a simple three-step synthesis of naphtho[2,1-b:7,8-b ']bis[1]benzothiophene, which is scalable to multi-hundred-gram. We report the subsequent functionalization of this compound into iodine, boronic ester and silane derivatives, which are useful intermediates for various applications. The core structure was analyzed by NMR and single-crystal X-ray diffraction, and the physical properties were investigated by cyclic voltammetry, UV/Vis- and fluorescence spectroscopy.
| Item Type: | Article |
|---|---|
| Uncontrolled Keywords: | ARYL HALIDES; SULFOXIDES; OXIDATION; SULFIDES; Building blocks; Organic electronics; Sulfur heterocycles; Synthetic methods; Upscaling |
| Subjects: | 500 Science > 540 Chemistry & allied sciences |
| Divisions: | Chemistry and Pharmacy > Institut für Organische Chemie > Lehrstuhl Prof. Dr. Burkhard König |
| Depositing User: | Petra Gürster |
| Date Deposited: | 07 Apr 2020 09:36 |
| Last Modified: | 07 Apr 2020 09:36 |
| URI: | https://pred.uni-regensburg.de/id/eprint/25671 |
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