Controlled preparation of hollow zinc oxide microspheres from aqueous solution using hexamethylenetetramine and cysteine

Weinzierl, Daniel and Touraud, Didier and Lecker, Alois and Pfitzner, Arno and Kunz, Werner (2008) Controlled preparation of hollow zinc oxide microspheres from aqueous solution using hexamethylenetetramine and cysteine. MATERIALS RESEARCH BULLETIN, 43 (1). pp. 62-67. ISSN 0025-5408,

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Abstract

Zinc oxide particles were synthesized by precipitation from an aqueous solution of zinc nitrate tetrahydrate, R-(+)-cysteine and hexamethylenetetramine (HMTA, urotropine). Hollow microspheres of ZnO-cysteine hybrid material with a diameter of ca. 1 mu m and a wall thickness ca. 50 nm were obtained. After heating up to 850 degrees C pure ZnO microspheres of roughly the same size were formed. The particles were characterized by XRD, SEM, FT-IR and TGA. (c) 2007 Elsevier Ltd. All rights reserved.

Item Type: Article
Uncontrolled Keywords: ROOM-TEMPERATURE; ZNO PARTICLES; MORPHOLOGIES; COMPLEXES; amorphous materials; composites; oxides; crystal growth; X-ray diffraction
Subjects: 500 Science > 540 Chemistry & allied sciences
Divisions: Chemistry and Pharmacy > Institut für Anorganische Chemie > Chair Prof. Dr. Arno Pfitzner
Chemistry and Pharmacy > Institut für Physikalische und Theoretische Chemie > Chair of Chemistry VI - Physical Chemistry (Solution Chemistry) > Prof. Dr. Werner Kunz
Depositing User: Dr. Gernot Deinzer
Date Deposited: 11 Nov 2020 06:18
Last Modified: 11 Nov 2020 06:18
URI: https://pred.uni-regensburg.de/id/eprint/31513

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