Ritscher, Anna and Schlosser, Marc and Pfitzner, Arno and Lerch, Martin (2016) Study of the mechanochemical process to crystalline Cu2ZnSnS4 powder. MATERIALS RESEARCH BULLETIN, 84. pp. 162-167. ISSN 0025-5408, 1873-4227
Full text not available from this repository. (Request a copy)Abstract
Kesterite-type Cu2ZnSnS4 was synthesized from the corresponding binary sulfides by a mechanochemical route in a planetary ball mill. The reaction progress during this milling step was followed within a time range of 10-180 min by powder X-ray diffraction. In addition, the crystallization of the milled material was studied in situ by high-temperature X-ray diffraction methods in the temperature range of 300500 degrees C. Significant disorder (cation distribution) was observed at 500 degrees C, strongly decreasing during cooling down to ambient temperature with a rate of 60K/h. (C) 2016 Elsevier Ltd. All rights reserved.
| Item Type: | Article |
|---|---|
| Uncontrolled Keywords: | KESTERITE; TRANSITION; ABSORBER; Semiconductors; Chemical synthesis; X-ray diffraction; Crystal structure; Defects |
| Subjects: | 500 Science > 540 Chemistry & allied sciences |
| Divisions: | Chemistry and Pharmacy > Institut für Anorganische Chemie > Chair Prof. Dr. Arno Pfitzner |
| Depositing User: | Dr. Gernot Deinzer |
| Date Deposited: | 12 Apr 2019 07:25 |
| Last Modified: | 12 Apr 2019 07:25 |
| URI: | https://pred.uni-regensburg.de/id/eprint/3923 |
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