Meurer, Florian and von Essen, Carolina and Kuhn, Clemens and Puschmann, Horst and Bodensteiner, Michael (2022) The benefits of Cu K beta radiation for the single-crystal X-ray structure determination of crystalline sponges. IUCRJ, 9. pp. 349-354. ISSN 2052-2525
Full text not available from this repository. (Request a copy)Abstract
The crystalline sponge method facilitates the X-ray structure determination of samples that do not crystallize or are too sparsely available to afford viable crystallization. By including these materials in a metal-organic framework, the structure of the guest molecules can be determined. Some of the inherent difficulties of this method are discussed and the use of Cu K beta radiation is presented as a simple and effective means to improve the quality of the diffraction data that can be obtained from a sponge crystal.
| Item Type: | Article |
|---|---|
| Uncontrolled Keywords: | ABSOLUTE-CONFIGURATION; CRYSTALLOGRAPHY; DAMAGE; crystalline sponge; copper K beta radiation; metal-organic frameworks; X-ray analysis |
| Subjects: | 500 Science > 540 Chemistry & allied sciences |
| Divisions: | Chemistry and Pharmacy > Central Analytical Services |
| Depositing User: | Dr. Gernot Deinzer |
| Date Deposited: | 15 Feb 2024 14:36 |
| Last Modified: | 15 Feb 2024 14:36 |
| URI: | https://pred.uni-regensburg.de/id/eprint/57789 |
Actions (login required)
 |
View Item |
